3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

Base Information

Chemical Name:3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole
CAS No.:1417526-70-5
Molecular Formula:C₁₈H₁₅F₃N₆
Molecular Weight:372.353
Hs Code.:

Synonyms:3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

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Chemical Property of 3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

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Technology Process of 3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

There total 5 articles about 3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417526-67-0
4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole-3-thiol

: 1417526-70-5
3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; dihydrogen peroxide / water; dichloromethane / 1 h / 20 - 35 °C

2: 12 h / Reflux

3: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

With diphenyl phosphoryl azide; dihydrogen peroxide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 1417526-66-9
4'-(trifluoromethyl)biphenyl-4-carbohydrazide

: 1417526-70-5
3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 2.5 h / Reflux

1.2: 2 h / Reflux

2.1: acetic acid; dihydrogen peroxide / water; dichloromethane / 1 h / 20 - 35 °C

3.1: 12 h / Reflux

4.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

With diphenyl phosphoryl azide; dihydrogen peroxide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

: 1417526-68-1
4-ethyl-3-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

: 1417526-70-5
3-(azido methyl)-4-ethyl-5-(4'-(trifluoromethyl)biphenyl-4-yl)-4H-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 12 h / Reflux

2: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 3 h / Reflux

With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;