Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

Base Information

Chemical Name:Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester
CAS No.:200411-30-9
Molecular Formula:C₂₈H₃₇NO₅S
Molecular Weight:499.671
Hs Code.:

Synonyms:Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

Suppliers and Price of Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

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Technology Process of Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

There total 7 articles about Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80696-28-2,16397-19-6
(2R)-2-amino-2-butyl-1-ethanol

: 200411-30-9
Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NEt₃, 2.) NaH / 1.) THF, 0 deg C to r.t., 12 h, 2.) r.t., 1-2 weeks

2: BuLi / tetrahydrofuran; various solvent(s) / 1.) -78 deg C, 2.) -78 deg C to r.t., 12 h

3: BF₃*OEt₂ / methanol; CH₂Cl₂ / 12 h / Ambient temperature

4: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

5: 1.) THF, Me₂N(CH₂)2NMe₂, -78 deg C, 40 min, 2.) -78 deg C to r.t., 12 h

With pyridine; n-butyllithium; boron trifluoride diethyl etherate; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/a706333d

Reference yield:

: 3112-85-4
methylphenylsulfonate

: 200411-30-9
Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: BuLi / tetrahydrofuran; various solvent(s) / 1.) -78 deg C, 2.) -78 deg C to r.t., 12 h

2: BF₃*OEt₂ / methanol; CH₂Cl₂ / 12 h / Ambient temperature

3: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

4: 1.) THF, Me₂N(CH₂)2NMe₂, -78 deg C, 40 min, 2.) -78 deg C to r.t., 12 h

With pyridine; n-butyllithium; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/a706333d

Reference yield:

: 98-88-4
benzoyl chloride

: 200411-30-9
Acetic acid (R)-2-benzenesulfonyl-4-benzoylamino-1-pent-4-enyl-octyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

2: 1.) THF, Me₂N(CH₂)2NMe₂, -78 deg C, 40 min, 2.) -78 deg C to r.t., 12 h

With pyridine; In dichloromethane;
DOI:10.1039/a706333d