benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

Base Information

Chemical Name:benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate
CAS No.:1419222-25-5
Molecular Formula:C₂₇H₃₀N₂O₅
Molecular Weight:462.546
Hs Code.:

Synonyms:benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

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Chemical Property of benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

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Technology Process of benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

There total 4 articles about benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1419222-24-4
(R)-benzyl allyl(3-(4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)carbamate

: 106-95-6
allyl bromide

: 1419222-25-5
benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

Guidance literature:: (R)-benzyl allyl(3-(4-benzyl-2-oxooxazolidin-3-yl)-3-oxopropyl)carbamate; With sodium hexamethyldisilazane; In tetrahydrofuran; at -40 ℃; for 1h;

allyl bromide; In tetrahydrofuran; at -78 - 0 ℃; for 3h;

Reference yield:

: 183888-16-6
3-(allyl((benzyloxy)carbonyl)amino)propanoic acid

: 1419222-25-5
benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; (R)-1-((benzyloxy)carbonyl)piperidine-3-carboxylic acid / dichloromethane / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -40 °C

2.2: 3 h / -78 - 0 °C

With sodium hexamethyldisilazane; N-ethyl-N,N-diisopropylamine; (R)-1-((benzyloxy)carbonyl)piperidine-3-carboxylic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 44981-87-5
ethyl 3-(prop-2-en-1-ylamino)propanoate

: 1419222-25-5
benzyl allyl((R)-2-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)pent-4-enyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 5 - 20 °C

2.1: lithium hydroxide monohydrate / water; methanol / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; (R)-1-((benzyloxy)carbonyl)piperidine-3-carboxylic acid / dichloromethane / 20 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -40 °C

4.2: 3 h / -78 - 0 °C

With lithium hydroxide monohydrate; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; (R)-1-((benzyloxy)carbonyl)piperidine-3-carboxylic acid; In tetrahydrofuran; methanol; dichloromethane; water;