Ethyl 3-(allylamino)propanoate

Base Information

• Chemical Name: Ethyl 3-(allylamino)propanoate
• CAS No.: 44981-87-5
• Molecular Formula: C8H15NO2
• Molecular Weight: 157.213
• Hs Code.: 2922499990
• Mol file: 44981-87-5.mol

Synonyms:3-Allylamino-propionsaeure-ethylester;3-allylaminopropionic acid ethyl ester;2-Allyl-7-thia-2-azaspiro<4.4>nonan-1,3-dion;2-allylamino-1-ethoxycarbonylethane;

Chemical Property of Ethyl 3-(allylamino)propanoate

Chemical Property:

• PSA: 38.33000
• LogP: 1.10610

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl 3-(allylamino)propanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 3-(allylamino)propanoate

There total 3 articles about Ethyl 3-(allylamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-amino-2-propene (107-11-9,30551-89-4) + ethyl acrylate (140-88-5,9003-32-1) → ethyl 3-(prop-2-en-1-ylamino)propanoate (44981-87-5)

Guidance literature:

In ethanol; at 20 ℃; for 48h;

DOI:10.1016/j.tetlet.2012.01.001

Reference yield: 70.0%

1-amino-2-propene (107-11-9,30551-89-4) + ethyl acrylate (140-88-5,9003-32-1) → Bis(carbethoxyethyl)allylamine (4046-08-6) + ethyl 3-(prop-2-en-1-ylamino)propanoate (44981-87-5)

Guidance literature:

With aluminum oxide; In neat (no solvent); at 45 ℃; for 3h; Green chemistry;

DOI:10.3390/molecules21060815

Reference yield:

1-amino-2-propene (107-11-9,30551-89-4) + acrylic acid (79-10-7) → ethyl 3-(prop-2-en-1-ylamino)propanoate (44981-87-5)

Guidance literature:

DOI:10.1016/S0040-4020(01)86134-2

upstream raw materials:

1-amino-2-propene

ethyl acrylate

acrylic acid

Downstream raw materials:

2-(N-allyl-N-phenoxycarbonylamino)-1-ethoxycarbonylethane

4-{(E)-2-[Allyl-(2-ethoxycarbonyl-ethyl)-carbamoyl]-propenyl}-benzoic acid benzyl ester

allyl-[3-(4-benzyl-2-oxo-oxazolidin-3-yl)-3-oxo-propyl]-carbamic acid tert-butyl ester

(R)-3-((R)-4-Benzyl-2-oxo-oxazolidine-3-carbonyl)-2,3,4,7-tetrahydro-azepine-1-carboxylic acid tert-butyl ester

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