N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Base Information

Chemical Name:N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
CAS No.:1527480-11-0
Molecular Formula:C₁₉H₃₀BNO₃
Molecular Weight:331.263
Hs Code.:

Synonyms:N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

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Technology Process of N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

There total 6 articles about N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 20383-28-2
N,N-diisopropyl benzamide

: 73183-34-3
bis(pinacol)diborane

: 1527480-11-0
N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; C₁₉H₁₃N₃O; potassium tert-butylate; In tetrahydrofuran; at 80 ℃; for 12h; Reagent/catalyst; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1002/anie.201809929

Reference yield: 72.0%

: 35306-66-2
N,N-diisopropyl 3-chlorobenzamide

: 73183-34-3
bis(pinacol)diborane

: 1527480-11-0
N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: With potassium acetate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tricyclohexylphosphine; In 1,4-dioxane; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c3cc47852a

Reference yield:

: 108-18-9
diisopropylamine

: 1527480-11-0
N,N-diisopropyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C / Inert atmosphere

2: bis(dibenzylideneacetone)-palladium⁽⁰⁾; tricyclohexylphosphine; potassium acetate / 1,4-dioxane / 24 h / 100 °C / Inert atmosphere

With potassium acetate; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tricyclohexylphosphine; In 1,4-dioxane; dichloromethane;
DOI:10.1039/c3cc47852a