4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid

Base Information

Chemical Name:4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid
CAS No.:645417-02-3
Molecular Formula:C₁₇H₁₆BrNO₅S
Molecular Weight:426.288
Hs Code.:

Synonyms:4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid

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Chemical Property of 4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid

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Technology Process of 4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid

There total 1 articles about 4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 645417-01-2
ethyl {4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxy}acetate

: 645417-02-3
4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid

Guidance literature:: ethyl {4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxy}acetate; With potassium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 0.75h;

With hydrogenchloride; In water; pH=2;

Reference yield: 79.0%

: 645417-02-3
4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid

: 5720-07-0
4-methoxyphenylboronic acid

: (4-{[5-(4-methoxyphenyl)-2,3-dihydro-1H-indol-1-yl]sulfonyl}-2-methylphenoxy)-acetic acid

Guidance literature:: 4-[(5-bromo-2,3-dihydro-1H-indol-1-yl)sulfonyl]-2-methylphenoxyacetic acid; 4-methoxyphenylboronic acid; With sodium carbonate; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 60 ℃;

With trifluoroacetic acid; In 1,2-dimethoxyethane; water; pH=<= 4;