1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

Base Information

Chemical Name:1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene
CAS No.:944936-29-2
Molecular Formula:C₅₁H₇₇ClO₂S
Molecular Weight:789.69
Hs Code.:

Synonyms:1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

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Chemical Property of 1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

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Technology Process of 1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

There total 2 articles about 1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 52610-77-2
solanesyl bromide

: 14752-66-0
sodium p-chlorobenzenesulphinate

: 944936-29-2
1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1002/hlca.200790099

Reference yield:

: 13190-97-1,540-03-4
solanesol

: 944936-29-2
1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorous tribromide

2: 85 percent / dimethylformamide / 24 h / 20 °C

With phosphorus tribromide; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.200790099

Reference yield: 75.8%

: 944936-28-1
1-[(2E)-4-chloro-3-methylbut-2-enyl]-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methylbenzene

: 944936-29-2
1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene

: 944936-30-5
1-[(2E,6E,10E,14E,18E,22E,26E,30E,34E)-5-(4-chlorophenylsulfonyl)-3,7,11,15,19,23,27,31,35,39-decamethyltetraconta-2,6,10,14,18,22,26,30,34,38-decaenyl]-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methylbenzene

Guidance literature:: 1-chloro-4-[(2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethylhexatriaconta-2,6,10,14,18,22,26,30,34-nonaenylsulfonyl]benzene; With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -70 ℃; for 0.5h;

1-[(2E)-4-chloro-3-methylbut-2-enyl]-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methylbenzene; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -70 - 20 ℃; for 3h; Further stages.;
DOI:10.1002/hlca.200790099