2-(2-(2-Aminoethoxy)ethoxy)acetic acid hydrochloride

Base Information

• Chemical Name: 2-(2-(2-Aminoethoxy)ethoxy)acetic acid hydrochloride
• CAS No.: 134979-01-4
• Molecular Formula: C6H13NO4^.HCl
• Molecular Weight: 199.634
• Hs Code.: 2922509090
• Mol file: 134979-01-4.mol

Synonyms:Aceticacid, [2-(2-aminoethoxy)ethoxy]-, hydrochloride (9CI);

Chemical Property of 2-(2-(2-Aminoethoxy)ethoxy)acetic acid hydrochloride

Chemical Property:

• PSA: 81.78000
• LogP: 0.56520
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

2-(2-(2-Aminoethoxy)Ethoxy)AceticAcidHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2-(2-Aminoethoxy)ethoxy)acetic acid hydrochloride

There total 5 articles about 2-(2-(2-Aminoethoxy)ethoxy)acetic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butyloxycarbonyl)-8-amino-3,6-dioxaoctanoic acid (108466-89-3) → 2-(2-(2-amino-ethoxy)ethoxy)acetic acid hydrochloride (134979-01-4)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 0 ℃;

Reference yield:

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) → 2-(2-(2-amino-ethoxy)ethoxy)acetic acid hydrochloride (134979-01-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 58.3 g / sodium iodide / butan-2-one / 19 h / Heating

2: 16.7 g / dimethylformamide / 18 h / 95 °C

3: 1.1 g / Jones reagent / acetone / 0.5 h

4: 1.) hydrazine hydrate; 2.) cc. hydrochloric acid / 1.) methanol, reflux, 3 h; 2.) water

With hydrogenchloride; jones reagent; hydrazine hydrate; sodium iodide; In N,N-dimethyl-formamide; acetone; butanone;

DOI:10.1016/S0008-6215(00)85535-4

Reference yield:

2-[2-(2-iodoethoxy)ethoxy]ethanol (62573-16-4) → 2-(2-(2-amino-ethoxy)ethoxy)acetic acid hydrochloride (134979-01-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 16.7 g / dimethylformamide / 18 h / 95 °C

2: 1.1 g / Jones reagent / acetone / 0.5 h

3: 1.) hydrazine hydrate; 2.) cc. hydrochloric acid / 1.) methanol, reflux, 3 h; 2.) water

With hydrogenchloride; jones reagent; hydrazine hydrate; In N,N-dimethyl-formamide; acetone;

DOI:10.1016/S0008-6215(00)85535-4

upstream raw materials:

2-(2-(2-(1,3-dioxoisoindolin-2-yl)ethoxy)ethoxy)acetic acid

2-[2-(chloroethoxy)ethoxy]ethanol

2-[2-(2-iodoethoxy)ethoxy]ethanol

2-{2-[2-(2-hydroxyethoxy)ethoxy]ethyl}isoindole-1,3-dione

Downstream raw materials:

[2-[2-(2,5-dioxo-2,5-dihydropyrrol-1-yl)ethoxy]ethoxy] acetic acid

N-(tert-butyloxycarbonyl)-8-amino-3,6-dioxaoctanoic acid

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