cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en

Base Information

• Chemical Name: cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en
• CAS No.: 41065-77-4
• Molecular Formula: C₁₂H₂₂O₆S₂
• Molecular Weight: 326.435
• Mol file: 41065-77-4.mol

Synonyms:cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en

Chemical Property of cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en

There total 2 articles about cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2t-dimethyl-cyclohexa-3,5-diene-1r,2c-dicarboxylic acid-anhydride (41841-74-1) → cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en (41065-77-4)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran

2: Py

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1021/ja00788a023

Reference yield:

cis-1,2-Bis(hydroxymethyl)-1,2-dimethylcyclohex-4-en (41065-53-6) + methanesulfonyl chloride (124-63-0) → cis-1,2-Bis(methansulfonyloxymethyl)-1,2-dimethylcyclohex-4-en (41065-77-4)

Guidance literature:

With pyridine;

DOI:10.1021/ja00788a023

upstream raw materials:

cis-1,2-Bis(hydroxymethyl)-1,2-dimethylcyclohex-4-en

methanesulfonyl chloride

1,2t-dimethyl-cyclohexa-3,5-diene-1r,2c-dicarboxylic acid-anhydride