8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Base Information

Chemical Name:8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene
CAS No.:119794-28-4
Molecular Formula:C₂₃H₁₆Cl₂N₄
Molecular Weight:419.313
Hs Code.:

Synonyms:8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

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Technology Process of 8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

There total 3 articles about 8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2-Chloro-phenyl)-acetic acid N'-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-hydrazide

: 119794-28-4
8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: With acetic acid; Yield given; Heating;
DOI:10.1021/jm00126a003

Reference yield:

: 2444-36-2
2'-chloro-benzeneacetic acid

: 119794-28-4
8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,1'-carbonyldiimidazole / 1.) THF, 0 deg C, 2.a) 0 deg C, b) r.t.

2: AcOH / Heating

With acetic acid; 1,1'-carbonyldiimidazole;
DOI:10.1021/jm00126a003

Reference yield:

: 18091-89-9,112393-62-1
7-chloro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine

: 119794-28-4
8-Chloro-1-(2-chloro-benzyl)-6-phenyl-4H-2,3,5,10b-tetraaza-benzo[e]azulene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,1'-carbonyldiimidazole / 1.) THF, 0 deg C, 2.a) 0 deg C, b) r.t.

2: AcOH / Heating

With acetic acid; 1,1'-carbonyldiimidazole;
DOI:10.1021/jm00126a003