C₃₇H₄₈O₅Si

Base Information

Chemical Name:C₃₇H₄₈O₅Si
CAS No.:1391927-45-9
Molecular Formula:C₃₇H₄₈O₅Si
Molecular Weight:600.871
Hs Code.:

C<sub>37</sub>H<sub>48</sub>O<sub>5</sub>Si

Synonyms:C₃₇H₄₈O₅Si

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Chemical Property of C₃₇H₄₈O₅Si

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Technology Process of C₃₇H₄₈O₅Si

There total 7 articles about C₃₇H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391927-43-7
C₃₆H₄₆O₅Si

: 75-16-1
methylmagnesium bromide

: 1391927-45-9
C₃₇H₄₈O₅Si

Guidance literature:: C₃₆H₄₆O₅Si; methylmagnesium bromide; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol301795a

Reference yield:

: 92512-41-9
C₂₁H₂₈O₃Si

: 1391927-45-9
C₃₇H₄₈O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 - -55 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: 0.33 h / -78 °C / Inert atmosphere

3.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 5 h / 20 °C / Inert atmosphere

4.1: pyridinium p-toluenesulfonate / methanol / 22 h / 40 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

6.1: tetrahydrofuran / -78 °C / Inert atmosphere

6.2: 1 h / 20 °C / Molecular sieve; Inert atmosphere

With n-butyllithium; tetrapropylammonium perruthennate; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol301795a

Reference yield:

: 1391927-39-1
C₂₉H₃₆O₄Si

: 1391927-45-9
C₃₇H₄₈O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 - -55 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

1.3: 0.33 h / -78 °C / Inert atmosphere

2.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / methanol / 22 h / 40 °C / Inert atmosphere

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

5.1: tetrahydrofuran / -78 °C / Inert atmosphere

5.2: 1 h / 20 °C / Molecular sieve; Inert atmosphere

With n-butyllithium; tetrapropylammonium perruthennate; pyridinium p-toluenesulfonate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol301795a