2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

Base Information

Chemical Name:2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime
CAS No.:873692-56-9
Molecular Formula:C₂₀H₃₄N₂O₃SSi
Molecular Weight:410.653
Hs Code.:

Synonyms:2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

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Technology Process of 2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

There total 5 articles about 2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 873692-50-3
2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde oxime

: 18162-48-6
tert-butyldimethylsilyl chloride

: 873692-56-9
2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃;
DOI:10.1021/jo051652e

Reference yield:

: 1062368-90-4
4-methyl-N-(3-methylbut-2-en-1-yl)-N-(2-oxoethyl)benzenesulfonamide

: 873692-56-9
2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1.29 g / NH₂OH*HCl; NaHCO₃ / ethanol; H₂O / 20 °C

2: 95 percent / imidazole / dimethylformamide / 0 °C

With 1H-imidazole; hydroxylamine hydrochloride; sodium hydrogencarbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo051652e

Reference yield:

: 873692-63-8
methyl 2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetate

: 873692-56-9
2-[N-(3-methylbut-2-enyl)-N-tosylamino]acetaldehyde O-tert-butyldimethylsilyloxime

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / diethyl ether; hexane / -78 °C

2: 1.29 g / NH₂OH*HCl; NaHCO₃ / ethanol; H₂O / 20 °C

3: 95 percent / imidazole / dimethylformamide / 0 °C

With 1H-imidazole; hydroxylamine hydrochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; In diethyl ether; ethanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo051652e