2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

Base Information

Chemical Name:2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid
CAS No.:77745-75-6
Molecular Formula:C₂₂H₂₆Cl₄N₂O₂
Molecular Weight:492.273
Hs Code.:

Synonyms:2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

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Chemical Property of 2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

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Technology Process of 2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

There total 1 articles about 2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 23853-76-1
1-chloro-4-(3-methylbut-2-en-1-yl)benzene

: 77745-75-6
2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

Guidance literature:: With hydrogenchloride; isopentyl nitrite; at 0 - 5 ℃; for 0.25h;

Reference yield: 71.0%

: 77745-75-6
2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

: 77745-78-9
(E)-3-Amino-1-(4-chlorphenyl)-3-methyl-2-butanon-oxim

Guidance literature:: With ammonia; In ethanol; at 50 - 60 ℃; for 3h;

Reference yield:

: 77745-75-6
2,2'-Dichlor-1,1'-bis<(4-chlorphenyl)methyl>-2,2'-dimethylazopropan-N,N'-dioxid

: 77745-81-4
4-<(4-Chlorphenyl)methyl>-5,5-dimethyl-2-oxo-3-imidazolin-3-oxid

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / NH₃ / ethanol / 3 h / 50 - 60 °C

2: 67 percent / 1) triethylamine / diethyl ether / 2) 15h, room temperature

With ammonia; triethylamine; In diethyl ether; ethanol;