1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

Base Information

Chemical Name:1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil
CAS No.:100682-85-7
Molecular Formula:C₃₄H₃₉N₅O₉
Molecular Weight:661.712
Hs Code.:

Synonyms:1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

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Chemical Property of 1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

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Technology Process of 1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

There total 7 articles about 1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 100682-90-4
1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-5'-cyano-2',3'-cyclohexylidene-α-L-talo-furanosyl>uracil

: 100682-85-7
1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; for 0.5h; Heating;
DOI:10.1021/jo00362a027

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 100682-85-7
1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 18 h / 25 °C

2: acetic acid / H₂O / 5 h

With acetic acid; In methanol; water;
DOI:10.1021/jo00362a027

Reference yield:

: 34311-30-3
2',3'-O-cyclohexylideneuridine 5'-aldehyde

: 100682-85-7
1-<5'-(L-carbobenzyloxyphenylalanylmethylamino)-5'-deoxy-2',3'-O-cyclohexylidene-β-D-allo-furanosyluronic acid amide>uracil

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 3A sieves / tetrahydrofuran / 2 h / Ambient temperature

2: methanol / 18 h / 25 °C

3: acetic acid / H₂O / 5 h

With 3 A molecular sieve; acetic acid; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo00362a027