benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

Base Information

Chemical Name:benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester
CAS No.:174538-92-2
Molecular Formula:C₃₈H₄₆N₂O₉
Molecular Weight:674.791
Hs Code.:

Synonyms:benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

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Chemical Property of benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

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Technology Process of benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

There total 7 articles about benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 174538-91-1
L-valyl D-α-hydroxyhydrocinnamic acid t-butyl ester

: 174538-90-0
benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamic acid

: 174538-92-2
benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 12h;
DOI:10.1016/0040-4020(95)00964-7

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 174538-92-2
benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / dimethylaminopyridine, DCC / CH₂Cl₂ / 24 h / Ambient temperature

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 12 h

3: 92 percent / dimethylaminopyridine, DCC / CH₂Cl₂ / 12 h / 0 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/0040-4020(95)00964-7

Reference yield:

: 111505-52-3
D-α-hydroxyhydrocinnamic acid t-butyl ester

: 174538-92-2
benzyloxycarbonyl D-alanyl L-α-hydroxyhydrocinnamyl L-valyl D-α-hydroxy hydrocinnamic acid t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / dimethylaminopyridine, DCC / CH₂Cl₂ / 24 h / Ambient temperature

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 12 h

3: 92 percent / dimethylaminopyridine, DCC / CH₂Cl₂ / 12 h / 0 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/0040-4020(95)00964-7