4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine

Base Information

• Chemical Name: 4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine
• CAS No.: 80161-98-4
• Molecular Formula: C₃₂H₂₉Cl₂N₃O₄
• Molecular Weight: 590.506

Synonyms:4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine

Chemical Property of 4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine

Chemical Property:

Purity/Quality:

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Technology Process of 4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine

There total 2 articles about 4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

2,3,5-tri-O-benzyl-α- and β-D-arabinofuranosyl chlorides (52554-29-7) + 4,6-dichloro-1H-imidazo<4,5-c>pyridine (2589-12-0) → 3-((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-4,6-dichloro-3H-imidazo[4,5-c]pyridine + 4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine (80161-98-4) + 4,6-dichloro-1-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)imidazo<4,5-c>pyridine (80161-98-4)

Guidance literature:

With 4 A molecular sieve; In 1,2-dichloro-ethane; Yield given; Heating;

DOI:10.1021/jm00343a021

Reference yield: 37.0%

2,3,5-tri-O-benzyl-α- and β-D-arabinofuranosyl chlorides (52554-29-7) + 4,6-dichloro-1H-imidazo<4,5-c>pyridine (2589-12-0) → 3-((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-4,6-dichloro-3H-imidazo[4,5-c]pyridine + 4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine (80161-98-4) + 4,6-dichloro-1-(2,3,5-tri-O-benzyl-α-D-arabinofuranosyl)imidazo<4,5-c>pyridine (80161-98-4)

Guidance literature:

With 4 A molecular sieve; In 1,2-dichloro-ethane; Yield given; Heating;

DOI:10.1021/jm00343a021

Reference yield: 48.0%

4,6-dichloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine (80161-98-4) → 4-amino-6-chloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine (80161-97-3)

Guidance literature:

With ammonia; at 140 ℃; for 96h;

DOI:10.1021/jm00343a021

upstream raw materials:

2,3,5-tri-O-benzyl-α- and β-D-arabinofuranosyl chlorides

4,6-dichloro-1H-imidazo<4,5-c>pyridine

Downstream raw materials:

4-amino-6-chloro-1-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)imidazo<4,5-c>pyridine

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