5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

Base Information

Chemical Name:5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose
CAS No.:130469-49-7
Molecular Formula:C₂₄H₂₄O₉
Molecular Weight:456.449
Hs Code.:

Synonyms:5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

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Chemical Property of 5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

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Technology Process of 5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

There total 10 articles about 5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: C₂₀H₂₀O₇

: 130469-49-7
5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

Guidance literature:: With pyridine; Yield given; Ambient temperature;
DOI:10.1021/jm00105a054

Reference yield:

: 69827-90-3
5-O-benzoyl-3-C-benzoyloxymethyl-3-deoxy-1,2-O-isopropylidene-α-D-ribo-pentofuranose

: 130469-49-7
5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: aq. formic acid / 2 h / 55 °C

2: pyridine / 18 h / 20 °C

With pyridine; formic acid;
DOI:10.1081/NCN-200059338

Reference yield:

: 75783-45-8
(3aR,5R,6aS)-5-[[(tert-butyldiphenylsilyl)oxy]methyl]-2,2-dimethyltetrahydro-2H-furo[2,3-d][1,3]dioxol-6-one

: 130469-49-7
5-O-benzoyl-3-deoxy-3-<(benzoyloxy)methyl>-1,2-di-O-acetyl-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane / 0.5 h / 50 °C

1.2: 1.33 h / 50 °C

2.1: borane-THF / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 20 °C

4.1: pyridine / 1.67 h / 0 - 20 °C

5.1: trifluoroacetic acid / water / 1.5 h / 20 °C

6.1: dmap; pyridine / 2 h / 20 °C / Inert atmosphere

With pyridine; dmap; borane-THF; tetrabutyl ammonium fluoride; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; water;