O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

Base Information

Chemical Name:O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt
CAS No.:128060-25-3
Molecular Formula:C₆H₁₅N*C₂₆H₂₄ClN₂O₁₁PS
Molecular Weight:740.168
Hs Code.:

Synonyms:O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

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Chemical Property of O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

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Technology Process of O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

There total 2 articles about O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: O-(2-chlorophenyl)-bis-triethylammonium phosphorothioate

: 128060-22-0
3-N-benzoyl-2',3'-di-O-acetyl-5'-O-(methanesulfonyl)uridine

: 128060-25-3
O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1016/S0040-4020(01)89215-2

Reference yield:

: 105953-54-6
N³-benzoyl-2',3'-di-O-acetyl uridine

: 128060-25-3
O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine / 2 h / 20 °C

2: 46 percent / dimethylformamide / 96 h / 20 °C

In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89215-2

Reference yield: 89.0%

: 64-17-5
ethanol

: 128060-25-3
O-(2-chlorophenyl)-S-5'-(3-N-benzoyl-2',3'-di-O-acetyl-5'-deoxyuridyl)phosphorothioate triethyl ammonium salt

: 128060-44-6,128060-65-1
O-(2-chlorophenyl)-O-ethyl-S-(5'-deoxy-3-N-benzoyl-2',3'-di-O-acetyl-5'-uridyl)thiophosphate

Guidance literature:: With 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine; at 20 ℃; for 4h;
DOI:10.1016/S0040-4020(01)89215-2