(S)-N-ethoxycarbonyl-2-phenacylpiperidine

Base Information

Chemical Name:(S)-N-ethoxycarbonyl-2-phenacylpiperidine
CAS No.:205440-52-4
Molecular Formula:C₁₆H₂₁NO₃
Molecular Weight:275.348
Hs Code.:

Synonyms:(S)-N-ethoxycarbonyl-2-phenacylpiperidine

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Chemical Property of (S)-N-ethoxycarbonyl-2-phenacylpiperidine

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Technology Process of (S)-N-ethoxycarbonyl-2-phenacylpiperidine

There total 7 articles about (S)-N-ethoxycarbonyl-2-phenacylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.6%

: 205440-51-3
(S)-N-ethoxycarbonyl-2-(2,2-ethylenedioxy-2-phenylethyl)piperidine

: 205440-52-4
(S)-N-ethoxycarbonyl-2-phenacylpiperidine

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 18h; Ambient temperature;

Reference yield:

: 125261-01-0
2-(2-phenyl-1,3-dioxolan-2-yl)acetaldehyde

: 205440-52-4
(S)-N-ethoxycarbonyl-2-phenacylpiperidine

Guidance literature:: Multi-step reaction with 7 steps

1: 91.4 percent / 3 Angstroem molecular sieves / CH₂Cl₂ / 18 h / Ambient temperature

2: 95.8 percent / magnesium / tetrahydrofuran / 48 h / 0 °C

3: 1 N hydrochloric acid / methanol / 2 h / Ambient temperature

4: sodium borohydride / methanol / 0.67 h / Ambient temperature

5: hydrogen / palladium hydroxide on carbon / methanol / 48 h / 2280 - 3040 Torr

6: diisopropylethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 4 h / Ambient temperature

7: 97.6 percent / 5percent hydrochloric acid / tetrahydrofuran / 18 h / Ambient temperature

With hydrogenchloride; dmap; sodium tetrahydroborate; 3 A molecular sieve; hydrogen; magnesium; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: (2R,9S)-9-(2,2-ethylenedioxy-2-phenylethyl)-2-phenyl-1-aza-4-oxabicyclo[4.3.0]nonane

: 205440-52-4
(S)-N-ethoxycarbonyl-2-phenacylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium borohydride / methanol / 0.67 h / Ambient temperature

2: hydrogen / palladium hydroxide on carbon / methanol / 48 h / 2280 - 3040 Torr

3: diisopropylethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 4 h / Ambient temperature

4: 97.6 percent / 5percent hydrochloric acid / tetrahydrofuran / 18 h / Ambient temperature

With hydrogenchloride; dmap; sodium tetrahydroborate; hydrogen; N-ethyl-N,N-diisopropylamine; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane;