1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

Base Information

Chemical Name:1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine
CAS No.:1415814-56-0
Molecular Formula:C₃₂H₄₀N₂O₈S
Molecular Weight:612.744
Hs Code.:

Synonyms:1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

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Chemical Property of 1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

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Technology Process of 1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

There total 3 articles about 1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 757195-64-5
1-(1,3-Benzodioxol-5-ylmethyl)-4-(4-hydroxylbenzyl)piperazine

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 1415814-56-0
1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

Guidance literature:: With potassium carbonate; In acetonitrile; at 90 ℃; for 8h;
DOI:10.1016/j.bmc.2012.10.038

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1415814-56-0
1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dichloromethane / 10 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 8 h / 90 °C

With potassium carbonate; potassium hydroxide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2012.10.038

Reference yield:

: 32231-06-4
1-Piperonylpiperazine

: 1415814-56-0
1-(1,3-benzodioxol-5-ylmethyl)-4-(4-(2-(2-(2-(4-methylbenzenesulfonyloxy)ethoxy)ethoxy)ethoxy)benzyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-dichloro-ethane / 2 h / 20 °C

1.2: 20 °C

2.1: potassium carbonate / acetonitrile / 8 h / 90 °C

With potassium carbonate; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmc.2012.10.038