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1-PIPERONYLPIPERAZINE Manufacturer/High quality/Best price/In stock
Cas No: 32231-06-4
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
1-(1,3-benzodioxol-5-ylmethyl)piperazine
Cas No: 32231-06-4
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
1-Piperonylpiperazine
Cas No: 32231-06-4
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
Pharmaceutical Grade CAS 32231-06-4 with competitive price
Cas No: 32231-06-4
USD $ 139.0-210.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
1-PIPERONYLPIPERAZINE 32231-06-4
Cas No: 32231-06-4
No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier
High Purity 1-PIPERONYLPIPERAZINE Manufacturer/High quality/Best price/In stock Cas No: 32231-06-4
Cas No: 32231-06-4
USD $ 1.0-3.0 / Gram 10 Gram 1000 Kilogram/Month Wuhan Monad Medicine Tech Co.,LTD Contact Supplier
5-MEO-NEPT FAB144 MDBP
Cas No: 32231-06-4
No Data 1 Kilogram 10000 Kilogram/Month Jilin Tely Imp.& Exp.Co., Ltd. Contact Supplier
1-PIPERONYLPIPERAZINE
Cas No: 32231-06-4
No Data No Data No Data Shandong Hanjiang Chemical Co., Ltd. Contact Supplier
1-PIPERONYLPIPERAZINE
Cas No: 32231-06-4
No Data 1 Gram 1 Metric Ton/Day Shanghai Run-Biotech Co., Ltd. Contact Supplier
1(1,3-BENZODIOXOL-5-YLMETHYL) PIPERAZINE
Cas No: 32231-06-4
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32231-06-4 Usage

Chemical Properties

white to yellow or yellow-brownish cryst. solid
InChI:InChI=1/C12H16N2O2/c1-2-11-12(16-9-15-11)7-10(1)8-14-5-3-13-4-6-14/h1-2,7,13H,3-6,8-9H2/p+2

32231-06-4 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (224952)  1-Piperonylpiperazine  97% 32231-06-4 224952-25G 1,079.91CNY Detail
Alfa Aesar (L15625)  1-Piperonylpiperazine, 97%    32231-06-4 25g 968.0CNY Detail
Alfa Aesar (L15625)  1-Piperonylpiperazine, 97%    32231-06-4 5g 281.0CNY Detail

32231-06-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name 1-(1,3-benzodioxol-5-ylmethyl)piperazine

1.2 Other means of identification

Product number -
Other names EINECS 250-968-5

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:32231-06-4 SDS

32231-06-4Synthetic route

piperazine
110-85-0

piperazine

piperonol
495-76-1

piperonol

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
In o-xylene at 150℃; for 30h; Inert atmosphere; Sealed tube;81%
With aluminum (III) chloride; water In acetonitrile at 20℃; Irradiation;41%
1-(1,3-benzodioxol-5-ylmethyl)-4-[(2-nitrophenyl)methyl]piperazine

1-(1,3-benzodioxol-5-ylmethyl)-4-[(2-nitrophenyl)methyl]piperazine

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
With hydrazine In 1,4-dioxane; water Inert atmosphere; UV-irradiation;80%
piperazine
110-85-0

piperazine

piperonal
120-57-0

piperonal

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In tert-butyl methyl ether at 13 - 18℃; High pressure;78%
piperazine
110-85-0

piperazine

5-(chloromethyl)-1,3-benzodioxole
20850-43-5

5-(chloromethyl)-1,3-benzodioxole

piperazine dihydrochloride
142-64-3

piperazine dihydrochloride

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
Stage #1: piperazine; piperazine dihydrochloride In ethanol at 65℃; for 1h;
Stage #2: 5-(chloromethyl)-1,3-benzodioxole In ethanol at 78℃; for 2h;
benzyl 4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazine-1-carboxylate

benzyl 4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazine-1-carboxylate

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 2h;
4-chloro-6-dimethylamino-3-methylisoxazolo[5,4-d]pyrimidine
724428-97-1

4-chloro-6-dimethylamino-3-methylisoxazolo[5,4-d]pyrimidine

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

6-dimethylamino-3-methyl-4-(3,4-methylenedioxybenzylpiperazino)isoxazolo[5,4-d]pyrimidine

6-dimethylamino-3-methyl-4-(3,4-methylenedioxybenzylpiperazino)isoxazolo[5,4-d]pyrimidine

Conditions
ConditionsYield
In tetrahydrofuran Heating;99%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

tert-butyl 4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazine-1-carboxylate
1233143-33-3

tert-butyl 4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazine-1-carboxylate

Conditions
ConditionsYield
With triethylamine In methanol at 20℃; for 1.5h; Inert atmosphere;99%
p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-tosylpiperazine
305859-64-7

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-tosylpiperazine

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 4.5h; Inert atmosphere;99%
carbon dioxide
124-38-9

carbon dioxide

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

C13H16N2O3

C13H16N2O3

Conditions
ConditionsYield
With hydrogen In methanol at 120℃; under 30003 Torr; for 24h; Autoclave;99%
dimethyl acetylenedicarboxylate
762-42-5

dimethyl acetylenedicarboxylate

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

tetramethyl 2,2'-(1,4-piperazindiyl)dimaleate
24726-53-2

tetramethyl 2,2'-(1,4-piperazindiyl)dimaleate

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 1h;98%
2-chloropyrimidine
1722-12-9

2-chloropyrimidine

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

piribedil
3605-01-4

piribedil

Conditions
ConditionsYield
With C50H61Cl2N3Pd; potassium tert-butylate In 1,4-dioxane at 100℃; for 2h;98%
With C48H55ClN2Pd; sodium t-butanolate In 1,2-dimethoxyethane at 20℃; for 16h; Inert atmosphere; Sealed tube;98%
With potassium carbonate In tetrahydrofuran for 2h; Reflux;44%
4,6-dichloro-2,8-bis(dimethylamino)-5-phenyl-5H-thiopyrano[2,3-d:6,5-d']dipyrimidine
259654-07-4

4,6-dichloro-2,8-bis(dimethylamino)-5-phenyl-5H-thiopyrano[2,3-d:6,5-d']dipyrimidine

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

6-chloro-2,8-bis(dimethylamino)-5-phenyl-4-(4-piperonylpiperazino)-5H-thiopyrano[2,3-d:6,5-d']dipyrimidine
259654-13-2

6-chloro-2,8-bis(dimethylamino)-5-phenyl-4-(4-piperonylpiperazino)-5H-thiopyrano[2,3-d:6,5-d']dipyrimidine

Conditions
ConditionsYield
In tetrahydrofuran Substitution; Heating;95%
p-tolylsulfinyl amide
6873-55-8

p-tolylsulfinyl amide

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

C19H22N2O3S

C19H22N2O3S

Conditions
ConditionsYield
With europium(III) trifluoromethanesulfonate In acetonitrile at 50℃; for 24h; Inert atmosphere; Schlenk technique;95%
acetic anhydride
108-24-7

acetic anhydride

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

1-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)ethanone

1-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)ethanone

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 13h; Inert atmosphere;94%
(3αS,5αS,9βS)-5α,9-dimethyl-3-methylene-3α,5,5α,9β-tetrahydronaphtho[1,2-β]furan-2,8(3H,4H)-dione
66726-11-2

(3αS,5αS,9βS)-5α,9-dimethyl-3-methylene-3α,5,5α,9β-tetrahydronaphtho[1,2-β]furan-2,8(3H,4H)-dione

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

(3aS,5aS,9bS)-3-(4-benzo[1,3]dioxol-5-ylmethylpiperazin-1-ylmethyl)-5a,9-dimethyl-3a,5,5a,9b-tetrahydro-3H,4H-naphtho[1,2-b]furan-2,8-dione
1217269-74-3

(3aS,5aS,9bS)-3-(4-benzo[1,3]dioxol-5-ylmethylpiperazin-1-ylmethyl)-5a,9-dimethyl-3a,5,5a,9b-tetrahydro-3H,4H-naphtho[1,2-b]furan-2,8-dione

Conditions
ConditionsYield
In methanol at 20℃; Michael reaction; stereospecific reaction;94%
acrylonitrile
107-13-1

acrylonitrile

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

3-[4-[(benzo[1,3]dioxol-5-yl)methyl]piperazin-1-yl]propionitrile
385371-21-1

3-[4-[(benzo[1,3]dioxol-5-yl)methyl]piperazin-1-yl]propionitrile

Conditions
ConditionsYield
With triethylammonium acetate at 25℃; for 0.0166667h; Aza-Michael reaction; chemoselective reaction;93%
With multi-walled carbon nanotubes-triethylammonium hydrogen phosphate composite at 25℃; for 0.0166667h; Michael Addition; Green chemistry;93%
With single-walled carbon nanotube-triethylammonium hydrogen phosphate ionic liquid at 25℃; for 0.0166667h;94 %Chromat.
1-benzyl-1H-pyrrole-2,5-dione
1631-26-1

1-benzyl-1H-pyrrole-2,5-dione

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

3-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)-1-benzylpyrrolidine-2,5-dione

3-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)-1-benzylpyrrolidine-2,5-dione

Conditions
ConditionsYield
With triethylamine; lithium chloride In tetrahydrofuran at 23℃; for 1.5h; chemoselective reaction;93%
6-(2-bromoacetyl)-3-methylbenzo[d]oxazol-2(3H)-one
79851-85-7

6-(2-bromoacetyl)-3-methylbenzo[d]oxazol-2(3H)-one

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

6-[2-(4-Benzo[1,3]dioxol-5-ylmethyl-piperazin-1-yl)-acetyl]-3-methyl-3H-benzooxazol-2-one

6-[2-(4-Benzo[1,3]dioxol-5-ylmethyl-piperazin-1-yl)-acetyl]-3-methyl-3H-benzooxazol-2-one

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane for 8h; Ambient temperature;92%
6-benzoyl-2(3H)-benzoxazolone
54903-12-7

6-benzoyl-2(3H)-benzoxazolone

formaldehyd
50-00-0

formaldehyd

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

3-(4-Benzo[1,3]dioxol-5-ylmethyl-piperazin-1-ylmethyl)-6-benzoyl-3H-benzooxazol-2-one

3-(4-Benzo[1,3]dioxol-5-ylmethyl-piperazin-1-ylmethyl)-6-benzoyl-3H-benzooxazol-2-one

Conditions
ConditionsYield
In methanol for 1h; Heating;92%
formaldehyd
50-00-0

formaldehyd

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-methylpiperazine
55500-12-4

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-methylpiperazine

Conditions
ConditionsYield
Stage #1: formaldehyd; 1-Piperonylpiperazine With sodium tris(acetoxy)borohydride; triethylamine In dichloromethane; water at 20℃; for 16.5h;
Stage #2: With sodium hydrogencarbonate In dichloromethane; water
92%
Cholesteryl chloroformate
7144-08-3

Cholesteryl chloroformate

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

cholest-5-en-3-yl 4-(1,3-benzodioxol-5-ylmethyl)-1-piperazinecarboxylate
1120327-24-3

cholest-5-en-3-yl 4-(1,3-benzodioxol-5-ylmethyl)-1-piperazinecarboxylate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere;92%
2,6-Dichloropyrimidine
3934-20-1

2,6-Dichloropyrimidine

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

piribedil
3605-01-4

piribedil

Conditions
ConditionsYield
With C34H52BrN3OPd In 1,4-dioxane at 90℃; for 3h; Inert atmosphere; Schlenk technique;92%
benzyl bromide
100-39-0

benzyl bromide

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzylpiperazine
414876-23-6

1-(benzo[d][1,3]dioxol-5-ylmethyl)-4-benzylpiperazine

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 18.5h; Inert atmosphere;91%
2-Benzoxazolinone
59-49-4

2-Benzoxazolinone

formaldehyd
50-00-0

formaldehyd

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

3-(4-Benzo[1,3]dioxol-5-ylmethyl-piperazin-1-ylmethyl)-3H-benzooxazol-2-one

3-(4-Benzo[1,3]dioxol-5-ylmethyl-piperazin-1-ylmethyl)-3H-benzooxazol-2-one

Conditions
ConditionsYield
In methanol for 1h; Heating;90%
3-(4-chlorobutyl)-1,2,3-benzotriazin-4(3H)-one
158659-66-6

3-(4-chlorobutyl)-1,2,3-benzotriazin-4(3H)-one

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

3-[4-(4-benzo[1,3]dioxol-5-ylmethyl-piperazin-1-yl)-butyl]-3H-benzo[d][1,2,3]triazin-4-one; hydrochloride

3-[4-(4-benzo[1,3]dioxol-5-ylmethyl-piperazin-1-yl)-butyl]-3H-benzo[d][1,2,3]triazin-4-one; hydrochloride

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 80 - 120℃; for 1.16667h; microwave irradiation;90%
2-chloro-N-(4,5-dihydro-1-methyl-[1,2,4]-triazolo[4,3-a]quinolin-7-yl)acet-amide
1064703-56-5

2-chloro-N-(4,5-dihydro-1-methyl-[1,2,4]-triazolo[4,3-a]quinolin-7-yl)acet-amide

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

C25H28N6O3
1064703-58-7

C25H28N6O3

Conditions
ConditionsYield
With sodium carbonate In methanol for 10h; Reflux;90%
7-chloro-1-(2,4-difluorophenyl)-1,4-dihydro-8-methyl-6-nitro-4-oxoquinolone-3-carboxylic acid
1146300-32-4

7-chloro-1-(2,4-difluorophenyl)-1,4-dihydro-8-methyl-6-nitro-4-oxoquinolone-3-carboxylic acid

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

7-(4-((benzo[d][1,3]dioxol-5-yl)methyl)piperazin-1-yl)-1-(2,4-difluorophenyl)-1,4-dihydro-8-methyl-6-nitro-4-oxoquinoline-3-carboxylic acid
1146300-53-9

7-(4-((benzo[d][1,3]dioxol-5-yl)methyl)piperazin-1-yl)-1-(2,4-difluorophenyl)-1,4-dihydro-8-methyl-6-nitro-4-oxoquinoline-3-carboxylic acid

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide Microwave irradiation;90%
6-(bromomethyl)-5-chloro-2-(thiophen-2-yl)-7,8-dihydroquinoline

6-(bromomethyl)-5-chloro-2-(thiophen-2-yl)-7,8-dihydroquinoline

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

6-((4-(benzo[d] [1,3]dioxol-5-ylmethyl)piperazinyl)methyl)-5-chloro-2-(thiophen-2-yl)-7,8-dihydroquinoline

6-((4-(benzo[d] [1,3]dioxol-5-ylmethyl)piperazinyl)methyl)-5-chloro-2-(thiophen-2-yl)-7,8-dihydroquinoline

Conditions
ConditionsYield
With potassium carbonate In acetone at 20℃; for 12h;90%
1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

thioctic acid-N-hydroxysuccinimide ester
40846-94-4

thioctic acid-N-hydroxysuccinimide ester

1-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)-5-(1,2-dithiolan-3-yl)pentan-1-one

1-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)-5-(1,2-dithiolan-3-yl)pentan-1-one

Conditions
ConditionsYield
In dichloromethane at 20℃; for 5h; Inert atmosphere;89%
4-Fluoronitrobenzene
350-46-9

4-Fluoronitrobenzene

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

1-benzo[1,3]dioxol-5-ylmethyl-4-(4-nitro-phenyl)-piperazine

1-benzo[1,3]dioxol-5-ylmethyl-4-(4-nitro-phenyl)-piperazine

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃;89%
N-(3-chloropropyl)isonicotinamide

N-(3-chloropropyl)isonicotinamide

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

N-(3-(4-(piperonyl)piperazin-1-yl)propyl)isonicotinamide

N-(3-(4-(piperonyl)piperazin-1-yl)propyl)isonicotinamide

Conditions
ConditionsYield
Stage #1: N-(3-chloropropyl)isonicotinamide With sodium iodide In acetonitrile at 70℃; for 0.5h;
Stage #2: 1-Piperonylpiperazine With potassium carbonate In acetonitrile at 70℃; for 24h;
89%
(R,2E,4E)-6-((tert-butyldimethylsilyl)oxy)-7-(3,4-dimethoxyphenyl)hepta-2,4-dienoic acid
1448848-29-0

(R,2E,4E)-6-((tert-butyldimethylsilyl)oxy)-7-(3,4-dimethoxyphenyl)hepta-2,4-dienoic acid

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

(R,2E,4E)-1-(4-(benzo[1,3]dioxol-5-ylmethyl)piperazin-1-yl)-6-((tert-butyldimethylsilyl)oxy)-7-(3,4-dimethoxyphenyl)-hepta-2,4-dien-1-one

(R,2E,4E)-1-(4-(benzo[1,3]dioxol-5-ylmethyl)piperazin-1-yl)-6-((tert-butyldimethylsilyl)oxy)-7-(3,4-dimethoxyphenyl)-hepta-2,4-dien-1-one

Conditions
ConditionsYield
Stage #1: (R,2E,4E)-6-((tert-butyldimethylsilyl)oxy)-7-(3,4-dimethoxyphenyl)hepta-2,4-dienoic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere;
Stage #2: 1-Piperonylpiperazine In N,N-dimethyl-formamide at 20℃; Inert atmosphere;
89%
1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

2-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)pyrazine

2-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)pyrazine

Conditions
ConditionsYield
With iodine; sodium acetate In acetonitrile at 70℃;89%
2-chloro-N-(4-sulfamoylbenzyl)acetamide
101167-02-6

2-chloro-N-(4-sulfamoylbenzyl)acetamide

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

2-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)-N-(4-sulfamoylbenzyl)acetamide

2-(4-(benzo[d][1,3]dioxol-5-ylmethyl)piperazin-1-yl)-N-(4-sulfamoylbenzyl)acetamide

Conditions
ConditionsYield
With sodium carbonate In N,N-dimethyl-formamide at 100 - 120℃; Reflux;89%
formaldehyd
50-00-0

formaldehyd

propargyl ether mycophenolate

propargyl ether mycophenolate

1-Piperonylpiperazine
32231-06-4

1-Piperonylpiperazine

mycophenoyl methyl ester-7-(butynyloxy-N-(piperonylpiperazine))

mycophenoyl methyl ester-7-(butynyloxy-N-(piperonylpiperazine))

Conditions
ConditionsYield
With copper(l) iodide In 1,4-dioxane at 120℃; for 1h;89%

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