2-CHLORO-5-NITRONICOTINIC ACID ETHYL ESTER

Base Information

Chemical Name:2-CHLORO-5-NITRONICOTINIC ACID ETHYL ESTER
CAS No.:151322-83-7
Molecular Formula:C8H7ClN2O4
Molecular Weight:230.61
Hs Code.:2933399090
Mol file:151322-83-7.mol

Synonyms:ethyl 2-chloro-5-nitropyridine-3-carboxylate

Suppliers and Price of 2-CHLORO-5-NITRONICOTINIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ethyl2-chloro-5-nitronicotinate
25mg
$ 45.00

SynQuest Laboratories
Ethyl 2-chloro-5-nitronicotinate 95.0%
5 g
$ 920.00

SynQuest Laboratories
Ethyl 2-chloro-5-nitronicotinate 95.0%
1 g
$ 240.00

SynQuest Laboratories
Ethyl 2-chloro-5-nitronicotinate 95.0%
500 mg
$ 200.00

Matrix Scientific
Ethyl 2-chloro-5-nitronicotinate 97%
500mg
$ 181.00

Matrix Scientific
Ethyl 2-chloro-5-nitronicotinate 97%
1g
$ 228.00

Crysdot
Ethyl2-chloro-5-nitronicotinate 95+%
5g
$ 425.00

Chemenu
Ethyl2-chloro-5-nitronicotinate 95%
5g
$ 401.00

Biosynth Carbosynth
2-Chloro-5-nitronicotinic acid
1 g
$ 225.00

Biosynth Carbosynth
2-Chloro-5-nitronicotinic acid
250 mg
$ 120.00

Total 30 raw suppliers

Chemical Property of 2-CHLORO-5-NITRONICOTINIC ACID ETHYL ESTER

Chemical Property:

Vapor Pressure:0.000137mmHg at 25°C
Refractive Index:1.562
Boiling Point:333.4 °C at 760 mmHg
Flash Point:155.4 °C
PSA：85.01000
Density:1.433 g/cm³
LogP:2.34310
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

Ethyl2-chloro-5-nitronicotinate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-5-NITRONICOTINIC ACID ETHYL ESTER

There total 8 articles about 2-CHLORO-5-NITRONICOTINIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 156896-54-7
ethyl 1,2-dihydro-5-nitro-2-oxo-3-pyridinecarboxylate

: 151322-83-7
ethyl 2-chloro-5-nitro-3-pyridinecarboxylate

Guidance literature:: With N,N-dimethyl-formamide; trichlorophosphate; In chlorobenzene; for 4h; Heating;
DOI:10.3987/COM-93-6556

Reference yield: 81.0%

: 151322-83-7
ethyl 2-chloro-5-nitro-3-pyridinecarboxylate

Guidance literature:

Reference yield:

: 609-71-2
2-hydroxy-3-carboxypyridine

: 151322-83-7
ethyl 2-chloro-5-nitro-3-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / nitric acid, sulfuric acid / 1.) RT, 16 h, 2.) from 50 deg C to 70 deg C, 1.5 h

2: thionyl chloride / dimethylformamide / 2 h / Heating

3: dimethylformamide

With thionyl chloride; sulfuric acid; nitric acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00070a012