3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

Base Information

Chemical Name:3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid
CAS No.:1021204-69-2
Molecular Formula:C₁₈H₂₇NO₆S
Molecular Weight:385.481
Hs Code.:

Synonyms:3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

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Chemical Property of 3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

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Technology Process of 3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

There total 7 articles about 3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1021374-21-9
C₂₂H₃₅NO₆S

: 1021204-69-2
3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;

Reference yield:

: 1186241-07-5
C₂₂H₂₆ClNO₆S

: 1021204-69-2
3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 874-63-5
3,5-dimethylmethoxybenzene

: 1021204-69-2
3-[[1-[(4-Methoxy-2,6-dimethyl-phenyl)sulfonyl]-piperidin-2-yl]-methoxy]-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid / dichloromethane / 0 °C

2: potassium carbonate / acetone / 50 °C

3: tetrabutyl-ammonium chloride; sodium hydroxide / water; toluene / 0 - 20 °C

4: trifluoroacetic acid / dichloromethane / 20 °C

With chlorosulfonic acid; tetrabutyl-ammonium chloride; potassium carbonate; trifluoroacetic acid; sodium hydroxide; In dichloromethane; water; acetone; toluene;