1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Base Information

Chemical Name:1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride
CAS No.:139577-11-0
Molecular Formula:C₁₇H₂₉ClO₃Si
Molecular Weight:344.954
Hs Code.:

Synonyms:1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Suppliers and Price of 1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

There total 3 articles about 1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 139577-10-9
N,N-dimethyl-N-<1-(2'-t-butyldimethylsilyloxymethyl-3',4'-dimethoxyphenyl)ethyl>amine

: 139577-11-0
1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Guidance literature:: With chloroformic acid ethyl ester; In tetrahydrofuran; at 0 ℃; for 3h;

Reference yield:

: 139577-08-5
N,N-dimethyl-N-(1-(3',4'-dimethoxyphenyl)ethyl)amine

: 139577-11-0
1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) THF, 0 deg C, 1 h, 2.) THF, 25 deg C, 24 h

2: 81 percent / diisopropylethylamine / dimethylformamide / 2 h / 25 °C

3: 96 percent / ethyl chloroformate / tetrahydrofuran / 3 h / 0 °C

With n-butyllithium; chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 139577-09-6
N,N-dimethyl-N-<1-(2'-hydroxymethyl-3',4'-dimethoxyphenyl)ethyl>amine

: 139577-11-0
1-<3',4'-dimethoxy-2'-(t-butyldimethylsilylmethyl)phenyl>ethyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / diisopropylethylamine / dimethylformamide / 2 h / 25 °C

2: 96 percent / ethyl chloroformate / tetrahydrofuran / 3 h / 0 °C

With chloroformic acid ethyl ester; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;