5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

Base Information

Chemical Name:5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester
CAS No.:449775-55-7
Molecular Formula:C₁₅H₁₉BrN₂O₃S
Molecular Weight:387.297
Hs Code.:

5-bromo-pentanethioic acid <i>S</i>-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

Synonyms:5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

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Chemical Property of 5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

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Technology Process of 5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

There total 4 articles about 5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 4509-90-4
5-bromovaleroyl chloride

: 449775-53-5
N-(2-mercaptobenzoyl)-L-alaninamide

: 449775-55-7
5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

Guidance literature:: In N,N-dimethyl acetamide; at 20 ℃; for 3h;
DOI:10.1016/S0968-0896(01)00392-3

Reference yield:

: 119-80-2
2,2'-dithiobenzoic acid

: 449775-55-7
5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / 1,3-diisopropylcarbodiimide / tetrahydrofuran; propan-2-ol / 4 h / 20 °C

2: 92 percent / triethylamine / dimethylformamide / 20 °C

3: 77 percent / tris(carboxyethyl)phosphine hydrochloride; triethylamine / dimethylformamide; H₂O / 1 h / 20 °C

4: 70 percent / N,N-dimethyl-acetamide / 3 h / 20 °C

With tris(carboxyethyl)phosphine hydrochloride; triethylamine; diisopropyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/S0968-0896(01)00392-3

Reference yield:

: 449775-52-4
N,N'-(2,2'-dithiobisbenzoyl)-bis-L-alaninamide

: 449775-55-7
5-bromo-pentanethioic acid S-[2-(1-carbamoyl-ethylcarbamoyl)-phenyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / tris(carboxyethyl)phosphine hydrochloride; triethylamine / dimethylformamide; H₂O / 1 h / 20 °C

2: 70 percent / N,N-dimethyl-acetamide / 3 h / 20 °C

With tris(carboxyethyl)phosphine hydrochloride; triethylamine; In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00392-3