(5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate

Base Information

Chemical Name:(5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate
CAS No.:1011243-04-1
Molecular Formula:C₃₉H₅₄IO₁₀P
Molecular Weight:840.73
Hs Code.:

Synonyms:(5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate

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Chemical Property of (5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate

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Technology Process of (5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate

There total 1 articles about (5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3095-95-2
diethylphosphonoacetic acid

: 1011243-19-8
(5S,6R,8E,10E,13S,15E)-1-hydroxy-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methylhexadeca-8,10,15-trien-7-one

: 1011243-04-1
(5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; methyl iodide; In dichloromethane; at 23 ℃; for 2h;
DOI:10.1021/jo7024515

Reference yield: 75.0%

: 1011243-04-1
(5S,6R,8E,10E,13S,15E)-16-iodo-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxohexadeca-8,10,15-trienyl 2-(diethoxyphosphoryl)acetate

: 185909-51-7
(E)-3-hydroxyprop-1-enylboronic acid

: 1011243-20-1
(5S,6R,8E,10E,13R,15E,17E)-19-hydroxy-5,13-bis(4-methoxybenzyloxy)-6-methyl-7-oxononadeca-8,10,15,17-tetraenyl 2-(diethoxyphosphoryl)acetate

Guidance literature:: With thallium (I) ethoxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; water; at 23 ℃; for 3h;
DOI:10.1021/jo7024515