3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

Base Information

Chemical Name:3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose
CAS No.:155585-25-4
Molecular Formula:C₁₇H₂₄O₇S
Molecular Weight:372.439
Hs Code.:

Synonyms:3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

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Chemical Property of 3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

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Technology Process of 3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

There total 5 articles about 3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 155585-24-3
3-O-benzyl-6-deoxy-1,2-isopropylidene-β-L-talofuranose

: 124-63-0
methanesulfonyl chloride

: 155585-25-4
3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

Guidance literature:: With pyridine; for 3h; Ambient temperature;
DOI:10.1246/bcsj.67.236

Reference yield:

: 57099-04-4
3-O-benzyl-1,2-O-isopropylidene-α-D-allofuranose

: 155585-25-4
3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) pyridine / 1.) 55 deg C, overnight, 2.) RT, 3 h

2: 97 percent / 80percent aq. AcOH / 3 h / 50 °C

3: 89 percent / CH₃ONa / methanol / 2 h / Ambient temperature

4: 97 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

5: 96 percent / pyridine / 3 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; sodium methylate; acetic acid; In methanol; diethyl ether;
DOI:10.1246/bcsj.67.236

Reference yield:

: 155585-34-5
(3aR,6R,6aR)-6-benzyloxy-2,2-dimethyl-5-[(2S)-oxiran-2-yl]tetrahydrofuro[2,3-d][1,3]dioxole

: 155585-25-4
3-O-benzyl-6-deoxy-1,2-isopropylidene-5-O-methylsulfonyl-β-L-talofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

2: 96 percent / pyridine / 3 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1246/bcsj.67.236