Azetidin-3-ylmethanol hydrochloride

Base Information

• Chemical Name: Azetidin-3-ylmethanol hydrochloride
• CAS No.: 928038-44-2
• Molecular Formula: C4H10ClNO
• Molecular Weight: 123.582
• Hs Code.: 2933990090
• Mol file: 928038-44-2.mol

Synonyms:3-(Hydroxymethyl)azetidinehydrochloride;azetidin-3-ylmethanol hydrochloride;Azetidin-3-ylmethanol hydrochloride (1:1);Azetidin-3-ylmethanolhydrochlorid(1:1);(azetidin-3-yl)methanol hydrochloride;

Chemical Property of Azetidin-3-ylmethanol hydrochloride

Chemical Property:

• PSA: 32.26000
• LogP: 0.32890
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C
• Sensitive.: Hygroscopic

Purity/Quality:

98%, ^*data from raw suppliers

3-Azetidinemethanol Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37-60

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Azetidinemethanol Hydrochloride is used in the synthesis of human rhinovirus inhibitors.

Technology Process of Azetidin-3-ylmethanol hydrochloride

There total 4 articles about Azetidin-3-ylmethanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.48%

3-hydroxymethyl-azetidine-1-carboxylic acid tert-butyl ester (142253-56-3) → 3-(hydroxymethyl)azetidine hydrochloride (928038-44-2)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 25 ℃; for 2h;

Reference yield: 84.0%

(1-benzylazetidin-3-yl)methanol (99025-94-2) → 3-(hydroxymethyl)azetidine hydrochloride (928038-44-2)

Guidance literature:

With hydrogen; palladium(II) hydroxide/carbon; In methanol; for 24h;

Reference yield:

1-diphenylmethyl-3-hydroxymethylazetidine (72351-36-1) → 3-(hydroxymethyl)azetidine hydrochloride (928038-44-2)

Guidance literature:

1-diphenylmethyl-3-hydroxymethylazetidine; With hydrogen; palladium hydroxide on carbon; In methanol; under 3000.3 Torr;

With hydrogenchloride; In ethyl acetate;

upstream raw materials:

1-diphenylmethyl-3-hydroxymethylazetidine

(1-benzylazetidin-3-yl)methanol

3-hydroxymethyl-azetidine-1-carboxylic acid tert-butyl ester

Downstream raw materials:

1-[(7-benzyloxymethyl-6-tert-butoxy-9-deazapurin-9-yl)methyl]azetidine-3-methanol

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