C₂₈H₄₂N₂OSi

Base Information

Chemical Name:C₂₈H₄₂N₂OSi
CAS No.:1278575-16-8
Molecular Formula:C₂₈H₄₂N₂OSi
Molecular Weight:450.74
Hs Code.:

C<sub>28</sub>H<sub>42</sub>N<sub>2</sub>OSi

Synonyms:C₂₈H₄₂N₂OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₄₂N₂OSi

Chemical Property:

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Technology Process of C₂₈H₄₂N₂OSi

There total 5 articles about C₂₈H₄₂N₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 994-30-9
triethylsilyl chloride

: 1278575-08-8
C₂₂H₂₈N₂O

: 1278575-16-8
C₂₈H₄₂N₂OSi

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.1021/jo1025833

Reference yield:

: 1278574-96-1
C₂₂H₂₆N₂O₃

: 1278575-16-8
C₂₈H₄₂N₂OSi

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; acetic acid; zinc / methanol; water / 3 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 0 °C

With 1H-imidazole; hydrogenchloride; acetic acid; zinc; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo1025833

Reference yield:

: 150367-10-5,78346-64-2
1-nitro-1-heptene

: 1278575-16-8
C₂₈H₄₂N₂OSi

Guidance literature:: Multi-step reaction with 3 steps

1: 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol / toluene / 20 °C / Inert atmosphere

2: hydrogenchloride; acetic acid; zinc / methanol; water / 3 h / 20 °C

3: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 0 °C

With 1H-imidazole; hydrogenchloride; copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol; 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; acetic acid; zinc; In methanol; water; N,N-dimethyl-formamide; toluene; 1: Friedel Crafts/Henry reaction;
DOI:10.1021/jo1025833