(4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

Base Information

Chemical Name:(4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide
CAS No.:1443224-09-6
Molecular Formula:C₂₅H₃₃NO₃
Molecular Weight:395.542
Hs Code.:

Synonyms:(4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

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Chemical Property of (4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

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Technology Process of (4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

There total 3 articles about (4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (Z)-N-(4-methoxybenzyl)-2-methylpenta-2,4-dien-1-amine

: 1443224-01-8
6-((1E,3E)-3,5-dimethylhexa-1,3-dien-1-yl)-2,2-dimethyl-4H-1,3-dioxin-4-one

: 1443224-09-6
(4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

Guidance literature:: With pyridinium p-toluenesulfonate; In toluene; at 110 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol401354a

Reference yield:

: 67065-88-7
(Z)-2-methylpenta-2,4-dien-1-ol

: 1443224-09-6
(4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 0.33 h / -10 °C / Inert atmosphere

2: tetrahydrofuran / 12 h / -10 - 23 °C / Inert atmosphere

3: pyridinium p-toluenesulfonate / toluene / 3 h / 110 °C / Inert atmosphere

With N-Bromosuccinimide; pyridinium p-toluenesulfonate; triphenylphosphine; In tetrahydrofuran; toluene;
DOI:10.1021/ol401354a

Reference yield:

: 1447829-96-0
(Z)-5-bromo-4-methylpenta-1,3-diene

: 1443224-09-6
(4E,6E)-N-(4-methoxybenzyl)-6,8-dimethyl-N-((Z)-2-methylpenta-2,4-dien-1-yl)-3-oxonona-4,6-dienamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / -10 - 23 °C / Inert atmosphere

2: pyridinium p-toluenesulfonate / toluene / 3 h / 110 °C / Inert atmosphere

With pyridinium p-toluenesulfonate; In tetrahydrofuran; toluene;
DOI:10.1021/ol401354a