(S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

Base Information

Chemical Name:(S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate
CAS No.:865469-49-4
Molecular Formula:C₁₇H₂₁NO₄
Molecular Weight:303.358
Hs Code.:

Synonyms:(S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

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Chemical Property of (S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

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Technology Process of (S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

There total 7 articles about (S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-39-0
benzyl bromide

: 51154-06-4
(S)-2,5-dihydropyrrole-1,2-dicarboxylic acid 1-tert-butyl ester

: 865469-49-4
(S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

Guidance literature:: With caesium carbonate; In DMF (N,N-dimethyl-formamide); at 0 - 25 ℃; for 24h;

Reference yield: 78.0%

: 1219136-27-2
(2S,4S)-2-benzyl 1-tert-butyl 4-iodopyrrolidine-1,2-dicarboxylate

: 865469-49-4
(S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

: 565185-32-2
N-Boc-4,5-dehydroproline benzyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2018.05.050

Reference yield: 63.0%

: 89813-47-8
N-(tert-butoxycarbonyl)-(2S,4R)-4-hydroxyproline benzyl ester

: 865469-49-4
(S)-2-benzyl 1-tert-butyl 1H-pyrrole-1,2(2H,5H)-dicarboxylate

Guidance literature:: N-(tert-butoxycarbonyl)-(2S,4R)-4-hydroxyproline benzyl ester; With ortho-nitrophenyl selenocyanate; tributylphosphine; In tetrahydrofuran; at 20 ℃; for 7h;

With dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1039/c8cc01493k