7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

Base Information

Chemical Name:7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide
CAS No.:126922-06-3
Molecular Formula:C₁₇H₁₆N₄OS
Molecular Weight:324.406
Hs Code.:

7<6-cyano-2-phenyl-cyclopenta <c> pyridyl> thioacetohydrazide

Synonyms:7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

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Chemical Property of 7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

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Technology Process of 7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

There total 6 articles about 7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 126922-10-9
(4-Cyano-1-phenyl-6,7-dihydro-5H-[2]pyrindin-3-ylsulfanyl)-acetic acid ethyl ester

: 126922-06-3
7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 5h; Heating;

Reference yield:

: 100-52-7
benzaldehyde

: 126922-06-3
7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / ammonium acetate / 5 h / Heating

2: 90 percent / P₂S₅ / pyridine / 10 h / Heating

3: 85 percent / NaOAc / ethanol / 6 h / Heating

4: 80 percent / hydrazine hydrate / ethanol / 5 h / Heating

With ammonium acetate; tetraphosphorus decasulfide; sodium acetate; hydrazine hydrate; In pyridine; ethanol;

Reference yield:

: 5407-83-0
ethyl 2-cyano-2-cyclopentylideneacetate

: 126922-06-3
7<6-cyano-2-phenyl-cyclopenta pyridyl> thioacetohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / ammonium acetate / 5 h / Heating

2: 90 percent / P₂S₅ / pyridine / 10 h / Heating

3: 85 percent / NaOAc / ethanol / 6 h / Heating

4: 80 percent / hydrazine hydrate / ethanol / 5 h / Heating

With ammonium acetate; tetraphosphorus decasulfide; sodium acetate; hydrazine hydrate; In pyridine; ethanol;