(2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

Base Information

Chemical Name:(2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate
CAS No.:1242056-08-1
Molecular Formula:C₂₇H₃₁O₈*F₆P
Molecular Weight:628.503
Hs Code.:

Synonyms:(2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

Suppliers and Price of (2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

Chemical Property:

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Technology Process of (2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

There total 3 articles about (2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 1464-96-6
ethyl 2,6-dimethoxybenzoate

: 1242056-08-1
(2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

Guidance literature:: 1,2,3-trimethoxybenzene; With n-butyllithium; In diethyl ether; hexane; for 24h; Inert atmosphere;

ethyl 2,6-dimethoxybenzoate; In diethyl ether; hexane; for 4h; Inert atmosphere;

With potassium hexafluorophosphate; hexafluorophosphoric acid; In methanol; Inert atmosphere;
DOI:10.1016/j.dyepig.2021.109924

Reference yield:

: 1466-76-8
2-6-dimethoxybenzoic acid

: 1242056-08-1
(2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 5 h / Reflux; Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / 24 h / Inert atmosphere

2.2: 4 h / Inert atmosphere

2.3: Inert atmosphere

With n-butyllithium; sulfuric acid; In diethyl ether; hexane;
DOI:10.1016/j.dyepig.2021.109924