bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

Base Information

Chemical Name:bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate
CAS No.:1242056-27-4
Molecular Formula:C₃₃H₄₅N₂O₆*F₆P
Molecular Weight:710.694
Hs Code.:

Synonyms:bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

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Chemical Property of bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

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Technology Process of bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

There total 4 articles about bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₂₇H₃₁O₈⁽¹⁺⁾*BF₄^(1-)

: 109-89-7
diethylamine

: 1242056-27-4
bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

Guidance literature:: With potassium hexafluorophosphate; In acetonitrile; for 18h; Heating;

Reference yield: 76.0%

: 1242056-08-1
(2,6-dimethoxyphenyl)-bis(2,4,6-trimethoxyphenyl)methylium hexafluorophosphate

: 109-89-7
diethylamine

: 1242056-27-4
bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

Guidance literature:: In acetonitrile; at 20 - 24 ℃;
DOI:10.1021/jo1009917

Reference yield:

: 1466-76-8
2-6-dimethoxybenzoic acid

: 1242056-27-4
bis(4-diethylamino-2, 6-dimethoxyphenyl)-(2,6-dimethoxyphenyl)-methylium hexafluorophosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 5 h / Reflux; Inert atmosphere

2.1: n-butyllithium / hexane; diethyl ether / 24 h / Inert atmosphere

2.2: 4 h / Inert atmosphere

2.3: Inert atmosphere

3.1: acetonitrile / 4 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

With n-butyllithium; sulfuric acid; In diethyl ether; hexane; acetonitrile;
DOI:10.1016/j.dyepig.2021.109924