Methyl 3-bromo-5-iodobenzoate

Base Information

• Chemical Name: Methyl 3-bromo-5-iodobenzoate
• CAS No.: 188813-07-2
• Molecular Formula: C8H6BrIO2
• Molecular Weight: 340.943
• Hs Code.: 2916399090
• Mol file: 188813-07-2.mol

Synonyms:3-Bromo-5-iodobenzoicacid methyl ester;Methyl 3-bromo-5-iodobenzoate;Methyl 5-bromo-3-iodobenzoate;

Chemical Property of Methyl 3-bromo-5-iodobenzoate

Chemical Property:

• Appearance/Colour: white crystal powder
• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 62.0-63.0 °C
• Refractive Index: 1.626
• Boiling Point: 334.458 °C at 760 mmHg
• Flash Point: 156.075 °C
• PSA: 26.30000
• Density: 2.059 g/cm³
• LogP: 2.84030

Purity/Quality:

97% ^*data from raw suppliers

Methyl3-Bromo-5-iodobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-bromo-5-iodobenzoate

There total 3 articles about Methyl 3-bromo-5-iodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-bromo-5-iodo-benzoic acid (188815-32-9) + methyl iodide (74-88-4) → methyl 3-bromo-5-iodobenzoate (188813-07-2)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 20h;

Reference yield:

3-bromo-5-iodo-benzoic acid (188815-32-9) → methyl 3-bromo-5-iodobenzoate (188813-07-2)

Guidance literature:

With hydrogenchloride; In methanol; diethyl ether; ethyl acetate;

Reference yield:

→ methyl 3-bromo-5-iodobenzoate (188813-07-2) + water (7732-18-5)

Guidance literature:

upstream raw materials:

3-bromo-5-iodo-benzoic acid

methyl iodide

Downstream raw materials:

3-bromo-5-iodobenzoic acid tert-butyl ester

t-butyl 3,5-diethynylbenzoate

t-butyl 3,5-di(trimethylsilylethynyl)benzoate

t-butyl 3,5-di(benzoylbiphenylethynyl)benzoate

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