4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide

Base Information

• Chemical Name: 4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide
• CAS No.: 300661-55-6
• Molecular Formula: C₁₇H₁₆ClN₃O₄S
• Molecular Weight: 393.851

Synonyms:4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide

Chemical Property of 4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide

Chemical Property:

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Technology Process of 4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide

There total 1 articles about 4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(4-methoxyphenoxy)acetic acid hydrazide (21953-91-3) + ammonium thiocyanate (1147550-11-5) + 4-chloro-benzoyl chloride (122-01-0) → 4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide (300661-55-6)

Guidance literature:

ammonium thiocyanate; 4-chloro-benzoyl chloride; With PEG-400; In dichloromethane; at 20 ℃; for 1h;

(4-methoxyphenoxy)acetic acid hydrazide; at 20 ℃; for 0.5h;

DOI:10.1080/00397910008086980

Reference yield: 87.0%

4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide (300661-55-6) → 2-(4-chlorobenzoylamino)-5-(4-methoxyphenyloxymethyl)-1,3,4-oxadiazole

Guidance literature:

With mercury(II) diacetate; In acetic acid; for 0.075h; microwave irradiation;

DOI:10.1081/SCC-100104342

Reference yield: 86.0%

4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbothioyl}-benzamide (300661-55-6) → 4-chloro-N-{N'-[(4-methoxy-phenoxy)-acetyl]-hydrazinocarbonyl}-benzamide

Guidance literature:

With potassium iodate; In water; for 0.5h; Heating;

DOI:10.1080/00397910008086980

upstream raw materials:

(4-methoxyphenoxy)acetic acid hydrazide

ammonium thiocyanate

4-chloro-benzoyl chloride

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