α-phenoxy>-α'-bromo-p-xylene

Base Information

Chemical Name:α-phenoxy>-α'-bromo-p-xylene
CAS No.:149704-57-4
Molecular Formula:C₄₅H₅₁BrO
Molecular Weight:687.803
Hs Code.:

α-<p-<tris(p-tert-butylphenyl)methyl>phenoxy>-α'-bromo-p-xylene

Synonyms:α-phenoxy>-α'-bromo-p-xylene

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Chemical Property of α-phenoxy>-α'-bromo-p-xylene

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Technology Process of α-phenoxy>-α'-bromo-p-xylene

There total 9 articles about α-phenoxy>-α'-bromo-p-xylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 623-24-5
1,4-bis(bromomethyl)benzene

: 143998-20-3
4-[tris-(4-tert-butylphenyl)methyl]phenol

: 149704-57-4
α-phenoxy>-α'-bromo-p-xylene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 20h; Ambient temperature;
DOI:10.1021/jo00066a030

Reference yield:

: 253185-03-4,253185-04-5
tert-butylbenzene

: 149704-57-4
α-phenoxy>-α'-bromo-p-xylene

Guidance literature:: Multi-step reaction with 3 steps

1: 6 percent

2: 97 percent / 20 h / 100 °C

3: 51 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature

With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00066a030

Reference yield:

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 149704-57-4
α-phenoxy>-α'-bromo-p-xylene

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Mg / 1) THF, 2 h, 2) THF, reflux, overnight

2: 94 percent / acetyl chloride / 48 h / Heating

3: 97 percent / 20 h / 100 °C

4: 51 percent / NaH / tetrahydrofuran / 20 h / Ambient temperature

With sodium hydride; magnesium; acetyl chloride; In tetrahydrofuran;
DOI:10.1021/jo00066a030