(4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

Base Information

Chemical Name:(4-benzyloxy-2-iodo-5-methoxyphenyl)methanol
CAS No.:169137-67-1
Molecular Formula:C₁₅H₁₅IO₃
Molecular Weight:370.187
Hs Code.:

Synonyms:(4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

Suppliers and Price of (4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

There total 3 articles about (4-benzyloxy-2-iodo-5-methoxyphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.7%

: 33693-48-0
4-benzyloxy-3-methoxybenzyl alcohol

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 169137-67-1
(4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

Guidance literature:: With ammonium cerium(IV) nitrate; tetra-(n-butyl)ammonium iodide; In acetonitrile; for 16h; Heating;
DOI:10.1002/ardp.19953280402

Reference yield:

: 33693-48-0
4-benzyloxy-3-methoxybenzyl alcohol

: 169137-67-1
(4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

Guidance literature:: With iodine; silver trifluoroacetate; In chloroform; at 22 ℃; for 2.16667h; Inert atmosphere;
DOI:10.1021/ol301154f

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 169137-67-1
(4-benzyloxy-2-iodo-5-methoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 °C / Inert atmosphere

2: iodine; silver trifluoroacetate / chloroform / 2.17 h / 22 °C / Inert atmosphere

With sodium tetrahydroborate; iodine; silver trifluoroacetate; In methanol; chloroform;
DOI:10.1021/ol301154f