4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

Base Information

Chemical Name:4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene
CAS No.:946570-44-1
Molecular Formula:C₂₀H₂₂O₅
Molecular Weight:342.392
Hs Code.:

Synonyms:4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

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Chemical Property of 4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

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Technology Process of 4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

There total 3 articles about 4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2211-94-1,26744-15-0
2,3-epoxypropyl p-methoxyphenyl ether

: 946570-44-1
4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / Heating

1.2: pyridinium chlorochromate; 4 Angstroem molecular sieves / CH₂Cl₂

2.1: 68 percent / p-toluenesulfonic acid*H₂O / benzene / 16 h / Heating

3.1: 80 percent / tBuOK / tetrahydrofuran / 19 h / Heating

With potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1021/jm0702579

Reference yield:

: 213828-28-5
1-(benzyloxy)-3-(4-methoxyphenoxy)acetone

: 946570-44-1
4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / p-toluenesulfonic acid*H₂O / benzene / 16 h / Heating

2: 80 percent / tBuOK / tetrahydrofuran / 19 h / Heating

With potassium tert-butylate; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1021/jm0702579

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 946570-44-1
4-methoxy-1-({4-methylene-2-[(phenylmethoxy)methyl](1,3-dioxolan-2-yl)}methoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / Heating

1.2: pyridinium chlorochromate; 4 Angstroem molecular sieves / CH₂Cl₂

2.1: 68 percent / p-toluenesulfonic acid*H₂O / benzene / 16 h / Heating

3.1: 80 percent / tBuOK / tetrahydrofuran / 19 h / Heating

With potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1021/jm0702579