(1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III)

Base Information

• Chemical Name: (1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III)
• CAS No.: 1361006-59-8
• Molecular Formula: C₂₃H₂₈IrN₃O₂
• Molecular Weight: 570.714

Synonyms:(1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III)

Chemical Property of (1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III)

Chemical Property:

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Technology Process of (1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III)

There total 1 articles about (1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)iridium(I) (1085473-84-2) + oxygen (80937-33-3) → (1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III) (1361006-59-8)

Guidance literature:

In benzene-d6; at 20 ℃; for 3h; Solvent; Temperature;

DOI:10.1021/ic302570s

Reference yield:

(1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III) (1361006-59-8) + triphenylphosphine (603-35-0) → Triphenylphosphine oxide (791-28-6)

Guidance literature:

Inert atmosphere;

DOI:10.1021/ic302570s

Reference yield:

carbon monoxide (201230-82-2) + (1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)peroxoiridium(III) (1361006-59-8) → 1,5-cis,cis-cyclooctadiene (1552-12-1,111-78-4) + [Ir(N,N-dimethyl-N′,N″-diphenylguanidinato)(CO)2] (1421969-72-3) + [Ir{N,N-dimethyl-N′,N″-diphenylguanidinato}(η4-1,5-cyclooctadiene)(carbonato-κ2O,O′)] (1421969-84-7)

Guidance literature:

In benzene-d6; at 20 ℃; for 24h;

DOI:10.1021/ic302570s

upstream raw materials:

(1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)iridium(I)

oxygen

Downstream raw materials:

1,5-cis,cis-cyclooctadiene

[Ir(N,N-dimethyl-N′,N″-diphenylguanidinato)(CO)₂]

[Ir{N,N-dimethyl-N′,N″-diphenylguanidinato}(η⁴-1,5-cyclooctadiene)(carbonato-κ²O,O′)]

(1,5-cyclooctadiene)(N,N-dimethyl-N′,N″-diphenylguanidinato)iridium(I)

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