{2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

Base Information

Chemical Name:{2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine
CAS No.:832724-00-2
Molecular Formula:C₂₇H₃₀N₄O
Molecular Weight:426.561
Hs Code.:

Synonyms:{2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

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Chemical Property of {2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

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Technology Process of {2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

There total 9 articles about {2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 832723-99-6
8-(benzyloxy)-2,4,5-trimethyl-1,5-dihydroimidazo[4,5-b]carbazole

: 4584-46-7
(2-chloroethyl)dimethylamine hydrochloride

: 832724-00-2
{2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

Guidance literature:: With adogene 464; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; for 16h; Heating;
DOI:10.1016/j.bmc.2004.09.047

Reference yield:

: 832723-88-3
7-amino-8-methyl-9H-carbazol-3-ol

: 832724-00-2
{2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

Guidance literature:: Multi-step reaction with 8 steps

1.1: 62 percent / 2 h / Heating

2.1: 64 percent / sodium hydride / dimethylformamide; various solvent(s) / 20 °C

3.1: 53 percent / nitric acid; acetic acid / 3 h / 20 °C

4.1: 100 percent / sodium hydroxide / ethanol; H₂O / 5 h / Heating

5.1: 78 percent / sodium hydride / dimethylformamide; various solvent(s) / 20 °C

6.1: 94 percent / hydrazine hydrate; nickel / tetrahydrofuran; methanol / Heating

7.1: triethylamine / tetrahydrofuran

7.2: 3.12 g / dimethylformamide / 4 h / Heating

8.1: 79 percent / potassium carbonate; adogene 464 / tetrahydrofuran; dimethylformamide / 16 h / Heating

With sodium hydroxide; adogene 464; nitric acid; nickel; sodium hydride; potassium carbonate; hydrazine hydrate; acetic acid; triethylamine; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.047

Reference yield:

: 832723-92-9
7-amino-8,9-dimethyl-6-nitro-9H-carbazol-3-ol

: 832724-00-2
{2-[8-(benzyloxy)-2,4,5-trimethylimidazo[4,5-b]carbazol-1(5H)-yl]ethy}dimethylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 78 percent / sodium hydride / dimethylformamide; various solvent(s) / 20 °C

2.1: 94 percent / hydrazine hydrate; nickel / tetrahydrofuran; methanol / Heating

3.1: triethylamine / tetrahydrofuran

3.2: 3.12 g / dimethylformamide / 4 h / Heating

4.1: 79 percent / potassium carbonate; adogene 464 / tetrahydrofuran; dimethylformamide / 16 h / Heating

With adogene 464; nickel; sodium hydride; potassium carbonate; hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.047