tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate

Base Information

• Chemical Name: tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate
• CAS No.: 1161932-64-4
• Molecular Formula: C₂₀H₂₂N₂O₅S
• Molecular Weight: 402.471

Synonyms:tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate

Chemical Property of tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate

There total 1 articles about tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C15H14N2O3S (1086383-97-2) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate (1161932-64-4)

Guidance literature:

C₁₅H₁₄N₂O₃S; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.0833333h;

di-tert-butyl dicarbonate; In tetrahydrofuran; mineral oil; at 0 - 20 ℃;

DOI:10.1021/jo900627a

Reference yield: 66.0%

tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate (1161932-64-4) + phenylmagnesium bromide (100-58-3) → C26H28N2O5S (1161932-67-7)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1021/jo900627a

Reference yield:

tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate (1161932-64-4) + (4-chlorphenyl)magnesium bromide (873-77-8) → C26H27ClN2O5S

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1021/jo900627a

upstream raw materials:

C₁₅H₁₄N₂O₃S

di-tert-butyl dicarbonate

Downstream raw materials:

C₂₆H₂₈N₂O₅S

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1161932-64-4 tert-butyl 1-(4-methoxybenzyl)-2,3-dihydro-2,5-dioxo-1H-thieno[3,2-e][1,4]diazepine-4(5H)-carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send