2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

Base Information

Chemical Name:2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile
CAS No.:1404291-51-5
Molecular Formula:C₂₅H₁₈N₂S
Molecular Weight:378.497
Hs Code.:

Synonyms:2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

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Technology Process of 2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

There total 2 articles about 2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 98546-51-1
(4-thiomethoxyphenyl)boronic acid

: 298212-99-4
2-(4-iodophenyl)-1,8a-dihydroazulene-1,1-dicarbonitrile

: 1404291-51-5
2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium fluoride dihydrate; In water; toluene; at 90 ℃; for 48h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/adfm.201200897

Reference yield:

: 1448895-68-8
C₂₅H₁₈N₂S

: 1404291-51-5
2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

Guidance literature:: Kinetics; Heating;
DOI:10.1002/adfm.201200897

Reference yield:

: 1404291-51-5
2-[4′-methylthio(1,1′-biphenyl)-4-yl]-1,8a-dihydroazulene-1,1-dicarbonitrile

: 1424657-54-4
2-[4′-methylthio(1,1′-biphenyl)-4-yl]-7,8-dibromo-1,7,8,8a-tetrahydroazulene-1,1-dicarbonitrile

Guidance literature:: With bromine; In dichloromethane; at -78 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1002/adfm.201200897