[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

Base Information

Chemical Name:[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde
CAS No.:85236-06-2
Molecular Formula:C₂₄H₃₄O
Molecular Weight:338.533
Hs Code.:

Synonyms:[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

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Chemical Property of [2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

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Technology Process of [2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

There total 4 articles about [2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85236-05-1
2-[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-ethanol

: 85236-06-2
[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

Guidance literature:: With manganese(IV) oxide; In Petroleum ether; at 0 ℃; for 1h; Yield given;
DOI:10.1021/ja00349a039

Reference yield:

: 85236-03-9
(7E)-12,20-tetramethylene-10,14-retro-retinyl tert-butyldimethylsilyl ether

: 85236-06-2
[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetra-n-butylammonium fluoride / tetrahydrofuran / 4.5 h

2: 5.4 percent

3: MnO₂ / light petroleum / 1 h / 0 °C

With manganese(IV) oxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; Petroleum ether;
DOI:10.1021/ja00349a039

Reference yield:

: 85236-04-0
2-{2-[(E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-1,2,4-trienyl]-cyclohept-1-enyl}-ethanol

: 85236-06-2
[2-[(2E,4E)-3-Methyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dien-(Z)-ylidene]-cyclohept-(E)-ylidene]-acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 5.4 percent

2: MnO₂ / light petroleum / 1 h / 0 °C

With manganese(IV) oxide; In Petroleum ether;
DOI:10.1021/ja00349a039