5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

Base Information

Chemical Name:5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone
CAS No.:148759-06-2
Molecular Formula:C₂₁H₂₂ClN₃O₃
Molecular Weight:399.877
Hs Code.:

Synonyms:5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

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Chemical Property of 5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

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Technology Process of 5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

There total 1 articles about 5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 92574-75-9
2-((benzyloxy)methyl)-4,5-dichloropyridazin-3(2H)-one

: 104-63-2
N-Benzylethanolamine

: 148759-06-2
5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

: 148759-08-4
4-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-5-chloro-3(2H)-pyridazinone

Guidance literature:: In toluene; for 11h; Heating;

Reference yield: 65.0%

: 148759-06-2
5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

: 148759-07-3
5-(N-benzyl-N-2-chloroethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

Guidance literature:: With dmap; thionyl chloride; In dichloromethane; for 5h; Heating;

Reference yield:

: 148759-06-2
5-(N-benzyl-N-2-hydroxyethylamino)-2-benzyloxymethyl-4-chloro-3(2H)-pyridazinone

: 7-benzyloxymethyl-3,4-dihydro-2H-pyridazino<4,5-b><1,4>oxazin-8(7H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / sodium ethoxide / ethanol / 11 h / Heating

2: 20 percent / 36percent aq. HCl, H₂ / 10percent Pd-C / methanol / 0.08 h / Ambient temperature

With hydrogenchloride; hydrogen; sodium ethanolate; palladium on activated charcoal; In methanol; ethanol;