(E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

Base Information

Chemical Name:(E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene
CAS No.:335003-93-5
Molecular Formula:C₂₄H₂₆Br₂I₂N₂O₄S₂
Molecular Weight:884.23
Hs Code.:

Synonyms:(E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

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Chemical Property of (E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

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Technology Process of (E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

There total 6 articles about (E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 821-06-7
(E)-1,4-dibromobutene

: 335004-32-5
(E)-N,N'-bis[(4-iodophenyl)sulfonyl]-2-butene-1,4-diamine

: 335003-93-5
(E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 80 ℃; for 17h;
DOI:10.1002/1099-0690(200101)2001:2<329::aid-ejoc329>3.0.co;2-n

Reference yield:

: 591-50-4
iodobenzene

: 335003-93-5
(E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

Guidance literature:: Multi-step reaction with 6 steps

1: chlorosulfonic acid / 20 °C

2: NH₃

3: 90 percent / Et₃N; DMAP / CH₂Cl₂

4: 92 percent / K₂CO₃ / dimethylformamide / 20 °C

5: 98 percent / trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

6: 40 percent / NaH / dimethylformamide / 17 h / 80 °C

With chlorosulfonic acid; dmap; ammonia; sodium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200101)2001:2<329::aid-ejoc329>3.0.co;2-n

Reference yield:

: 98-61-3
p-Iodobenzenesulfonyl chloride

: 335003-93-5
(E,E,E)-1,14-dibromo-N,N'-bis[(4-iodophenyl)sulfonyl]-5,10-diazatetradeca-2,7,12-triene

Guidance literature:: Multi-step reaction with 5 steps

1: NH₃

2: 90 percent / Et₃N; DMAP / CH₂Cl₂

3: 92 percent / K₂CO₃ / dimethylformamide / 20 °C

4: 98 percent / trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

5: 40 percent / NaH / dimethylformamide / 17 h / 80 °C

With dmap; ammonia; sodium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200101)2001:2<329::aid-ejoc329>3.0.co;2-n