C₃₁H₃₆ClNO₉

Base Information

Chemical Name:C₃₁H₃₆ClNO₉
CAS No.:1327166-00-6
Molecular Formula:C₃₁H₃₆ClNO₉
Molecular Weight:602.081
Hs Code.:

C<sub>31</sub>H<sub>36</sub>ClNO<sub>9</sub>

Synonyms:C₃₁H₃₆ClNO₉

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Chemical Property of C₃₁H₃₆ClNO₉

Chemical Property:

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Technology Process of C₃₁H₃₆ClNO₉

There total 13 articles about C₃₁H₃₆ClNO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1327165-99-0
C₂₈H₂₉ClO₁₀

: 765-30-0
Cyclopropylamine

: 1327166-00-6
C₃₁H₃₆ClNO₉

Guidance literature:: With sodium cyanoborohydride; acetic acid; In dichloromethane; acetonitrile; at 0 ℃;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 1185339-44-9
C₁₉H₂₁ClO₅

: 1327166-00-6
C₃₁H₃₆ClNO₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap / pyridine; dichloromethane / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

4.1: toluene-4-sulfonic acid / water; toluene / Reflux

5.1: ozone / dichloromethane

5.2: -78 - 20 °C

6.1: sodium cyanoborohydride; acetic acid / dichloromethane; acetonitrile / 0 °C

With dmap; aluminum (III) chloride; sodium tetrahydroborate; sodium cyanoborohydride; toluene-4-sulfonic acid; ozone; acetic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; toluene; acetonitrile; 2.1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 312749-31-8
2-chloro-5-bromobenzophenone

: 1327166-00-6
C₃₁H₃₆ClNO₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / Reflux

2.1: n-butyllithium / tetrahydrofuran; toluene / -78 °C

3.1: methanesulfonic acid / methanesulfonic acid / -78 - 20 °C

4.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -30 - -10 °C

5.1: dmap / pyridine; dichloromethane / 20 °C

6.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C

7.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

8.1: toluene-4-sulfonic acid / water; toluene / Reflux

9.1: ozone / dichloromethane

9.2: -78 - 20 °C

10.1: sodium cyanoborohydride; acetic acid / dichloromethane; acetonitrile / 0 °C

With triethylsilane; dmap; aluminum (III) chloride; sodium tetrahydroborate; n-butyllithium; methanesulfonic acid; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; sodium cyanoborohydride; toluene-4-sulfonic acid; ozone; acetic acid; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; methanesulfonic acid; dichloromethane; water; toluene; acetonitrile; 6.1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032