Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside

Base Information

Chemical Name:Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside
CAS No.:5329-58-8
Molecular Formula:C₁₈H₂₆O₁₀S
Molecular Weight:434.464
Hs Code.:
DSSTox Substance ID:DTXSID60276002
Nikkaji Number:J1.306.594B
Mol file:5329-58-8.mol

Synonyms:Phenyl-beta-galactopyranosyl-1,4-(1-thio-beta-D-glucopyranoside);Phenyl 1-thio-beta-lactoside;DTXSID60276002;Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside

Suppliers and Price of Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside

Chemical Property:

Vapor Pressure:8.66E-23mmHg at 25°C
Boiling Point:736.7°Cat760mmHg
Flash Point:399.4°C
Density:1.61g/cm³
XLogP3:-1.8
Hydrogen Bond Donor Count:7
Hydrogen Bond Acceptor Count:11
Rotatable Bond Count:6
Exact Mass:434.12466820
Heavy Atom Count:29
Complexity:507

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SC2C(C(C(C(O2)CO)OC3C(C(C(C(O3)CO)O)O)O)O)O
Isomeric SMILES:C1=CC=C(C=C1)S[C@H]2[C@@H]([C@H]([C@@H]([C@H](O2)CO)O[C@H]3[C@@H]([C@H]([C@H]([C@H](O3)CO)O)O)O)O)O

Technology Process of Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside

There total 8 articles about Phenyl 4-O-beta-D-galactopyranosyl-1-thio-beta-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4
1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose

: 27891-73-2,27894-87-7,5329-58-8
β-phenylsulfanyl lactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / BF₃*C₂H₅OC₂H₅ / CH₂Cl₂ / 24 h / 0 - 20 °C

2: NaOMe; IR resin (H+) / methanol

With IR resin (H+); boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2006.08.008

Reference yield:

: 108-98-5
thiophenol

: 27891-73-2,27894-87-7,5329-58-8
β-phenylsulfanyl lactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / boron trifluoride etherate / CH₂Cl₂ / 24 h / Ambient temperature

2: 100 percent / NaOMe / methanol / 12 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;
DOI:10.1248/cpb.43.1536

Reference yield:

: 108-98-5
thiophenol

: 27891-73-2,27894-87-7,5329-58-8
β-phenylsulfanyl lactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / BF₃*C₂H₅OC₂H₅ / CH₂Cl₂ / 24 h / 0 - 20 °C

2: NaOMe; IR resin (H+) / methanol

With IR resin (H+); boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2006.08.008