(1R,2S)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

Base Information

Chemical Name:(1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide
CAS No.:144609-75-6
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:

Synonyms:(1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

Chemical Property:

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Technology Process of (1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

There total 4 articles about (1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17680-04-5
(3,4-methylenedioxy)phenylmagnesium bromide

: 144609-75-6
(1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95.6 percent / tetrahydrofuran / 0.17 h / ice-cooling

2: 1) Et₃N, ethyl chloroformate, 2) NaN₃ / 1) acetone, ice-cooling, 0.5 h, 2) acetone, water, ice-cooling, 1 h

3: 16 h / Heating

With sodium azide; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00052a051

Reference yield:

: 935-79-5
cis-1,2,3,6-tetrahydrophthalic anhydride

: 144609-75-6
(1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95.6 percent / tetrahydrofuran / 0.17 h / ice-cooling

2: 1) Et₃N, ethyl chloroformate, 2) NaN₃ / 1) acetone, ice-cooling, 0.5 h, 2) acetone, water, ice-cooling, 1 h

3: 16 h / Heating

With sodium azide; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00052a051

Reference yield:

: 139025-41-5
(1R*,2S*)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenecarboxylic acid

: 144609-75-6
(1R*,2S*)-N-(tert-butoxycarbonyl)-2-<3',4'-(methylenedioxy)benzoyl>-4-cyclohexenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Et₃N, ethyl chloroformate, 2) NaN₃ / 1) acetone, ice-cooling, 0.5 h, 2) acetone, water, ice-cooling, 1 h

2: 16 h / Heating

With sodium azide; chloroformic acid ethyl ester; triethylamine;
DOI:10.1021/jo00052a051