Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

Base Information

Chemical Name:Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl
CAS No.:723242-25-9
Molecular Formula:C₃₁H₃₈ClN₃OPd
Molecular Weight:610.535
Hs Code.:

Synonyms:Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

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Chemical Property of Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

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Technology Process of Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

There total 2 articles about Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 723242-26-0
3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole

: 723242-25-9
Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane; acetonitrile

2: dichloromethane; acetonitrile

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/ja031587v

Reference yield:

: palladium dichloride

: 723242-26-0
3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole

: 723242-25-9
Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

Guidance literature:: With triethylamine; In acetonitrile; PdCl2 added to suspn. of ligand in MeCN, a few drops of triethylamine added, mixt. refluxed overnight; elem. anal.;
DOI:10.1021/ja031587v

Reference yield:

: 723242-25-9
Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole(1-)-κC2)Cl

: Pd(3-[N-2-pyridylmethyl-N-2-hydroxy-3,5-di(tert-butyl)benzylamino]ethylindole radical cation-,kappa.C₂)Cl⁽¹⁺⁾

Guidance literature:: With Ce⁽⁴⁺⁾; In N,N-dimethyl-formamide; oxidation in DMF at -60°C; not isolated, detected by UV spectroscopy;
DOI:10.1021/ja031587v